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Journal of Structural Chemistry

2016 year, number 6

Structure 3-methyl-2,3,4,4a, 5,10b-hexahydro-1H-spiro [chromeno [3,4-c] PYRIDINE-1,1'-CYCLOHEXANE] -2,4,5-trione

N.F. Kirillov, E.A. Nikiforova, M.V. Dmitriev, D.V. Baibarodskikh
Perm National Research State University, Perm, 614990 Russia
Keywords: рентгеноструктурный анализ, реакция Реформатского, N-метил-2-оксо-2Н-хромен-3-карбоксамид, метил-бромциклогексанкарбоксилат, спирохроменопиперидиндион, single crystal X-ray diffraction analysis, Reformatsky reaction, N-methyl-2-oxo-2Н-chromene-3-carboxamide, methyl bromo cyclohexane carboxylate, spiro chromeno piperidinedione

Abstract

By the interaction of methyl 1-bromo cyclohexane carboxylate with zinc and N-methyl-2-oxo-2Н-chromene-3-carboxyamide 3-methyl-2,3,4,4a,5,10b-hexahydro-1H-spiro[chromeno[3,4-c]pyridine-1,1-cyclohexane]-2,4,5-trione is obtained and its structure is determined by the single crystal X-ray diffraction analysis.