CRYSTAL AND MOLECULAR STRUCTURES OF 2-(4-CHLOROPHENYL)-5,7-DIMETHOXYQUINOLIN-4-YL PHENYL BIS(2-CHLOROETHYL) PHOSPHORAMIDATE
J.W. Yuan1, L.B. Qu2, X.L. Chen3, Z.B. Qu3, Y.C. Li1
1 Chemistry and Chemical Engineering School, Henan University of Technology
2 Chemistry and Chemical Engineering School, Henan University of Technology Department of Chemistry, Zhengzhou University, Key Laboratory of Organic Chemistry and Chemical Biology
3 Department of Chemistry, Zhengzhou University, Key Laboratory of Organic Chemistry and Chemical Biology
qulingbo@zzu.edu.cn
Ключевые слова: crystal and molecular structure, X-ray crystallography, 2-phenyl-4-quinolone, phosphoramidate
Страницы: 1015-1018
Аннотация
2-(4-chlorophenyl)-5,7-dimethoxyquinolin-4-yl phenyl bis(2-chloroethyl)phosphoramidate is synthesized and characterized by NMR, IR and single crystal X-ray crystallography. The crystal is triclinic, P1 space group, with a = 9.5188(19), b = 12.856(3), c = 13.250(3) Å, V =
= 1412.0(5) Å)3, and Z = 2 (at 291(2) K). The crystal packing arrangement indicates that the molecule is stacked through π…π aromatic stacking interactions.
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