CRYSTAL STRUCTURE OFВ N'–PIVALOYL–N–PHENYLPIVALOHYDRAZIDE
A. Saeed1, I. Arshad1, U. Florke2
1Quaid-I-Azam University, Islamabad, Pakistan
2Universitet Paderborn, Paderborn, Germany
Keywords: N'-pivaloyl-N-phenylpivalohydrazide, crystal structure
Abstract
A novel hydrazide compound (C16H24N2O2) is synthesized in a single step by the reaction of pivaloyl chloride with phenylhydrazine in a 2:1 molar ratio in dry DCM. The molecular structure is determined by the single crystal X-ray analysis. The compound crystallized in the monoclinic system, space group P21/c with a = 15.4638(17) Å, b = 9.9481(11) Å, c = 10.5276(12) Å, β = 90.194(3)°, Z = 4, V = 1619.5(3) Å3.
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