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Journal of Structural Chemistry

2013 year, number 2


Yu. R. Galina1, A. N. Lobov1, R. M. Sultanova1, L. V. Spirikhin1, V. A. Dokichev1, K. Yu. Suponitsky2
1Institute of Organic Chemistry, Ufa Scientific Center, Russian Academy of Sciences, Ufa
2A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, Moscow
Keywords: 5-diazo-exo-3-azatricyclo[ 2,6]decane-4-one, phosphazines, molecular structure, single crystal X‑ray diffraction study


The molecular structure of 5-[(triphenylphosphoranylidene)hydrazono]-exo-3-azatricyclo[]decane-4-one is determined. The C27H26N3OP compound crystallizes in the space group P-1: a = 9.2163(9) Å, b = 11.1102(11) Å, c = 11.9397(12) Å, α = 74.284(2)°, β = 78.532(2)°, γ = 72.004(2)°.