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Journal of Structural Chemistry

2013 year, number 2


O. N. Kazheva1, D. A. Rudakov2, G. V. Shilov1, O. A. D’yachenko1, V. I. Potkin2
1Institute of Problems of Chemical Physic, Russian Academy of Sciences, Chernogolovka, Russia
2Institute of Physical Organic Chemistry, National Academy of Sciences of Belarus, Minsk, Belarus
Keywords: halogenation, dicarba-nido-undecaborate, single-crystal X-ray diffraction analysis, nuclear magnetic resonance


A technique is proposed for directed synthesis of 6,11-dichloro-9-dimethylthio-7,8-dicarba- nido-undecaborane [6,11-Cl2-9-SMe2-7,8-С2В9Н9]. Single-crystal X-ray diffraction is used to identify the molecular and crystal structure of the compound.