MOLECULAR and CRYSTAL STRUCTURE of 4-trifluoro-2-[2-(4-fluorophenyl)hydrazine-1-ylidene]-1-(thiophen -2-YL)butane-1,3-dione
A. M. Magerramov, R. A. Alieva, V. I. Mardanova, F. M. Chyragov, A. V. Kurbanov, K. A. Potekhin
Keywords: single crystal X-ray diffraction, crystal structure, ?-diketone, 4-trifluoro-2-[2-(4-fluorophenyl)hydrazine-1-ylidene]-1-(thiophen-2-yl)butane-1, 3-dione
Pages: 205-208
Abstract
Single crystal X-ray diffraction is used to determine the crystal and molecular structure of 4-trifluoro-2-[2-(4-fluorophenyl)hydrazine-1-ylidene]-1-(thiophen-2-yl)butane-1,3-dione. Crystallographic data for C14H8F4N2O2S are as follows: a = 8.2723(6) Å, b = 9.3009(7) Å, c = 9.9895(7) Å; α = 79.224(2)°, β = 75.851(2)°, γ = 72.337(2)°. Triclinic crystal system, P-1 space group, dx = 1.622 g/cm3, V = 704.83(9) Å3, μ = 0.286 mm-1, crystal size 0.30×0.20×0.20 mm, R1 = 0.0891, wR2 = 0.1989.
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