Publishing House SB RAS:

Publishing House SB RAS:

Address of the Publishing House SB RAS:
Morskoy pr. 2, 630090 Novosibirsk, Russia



Advanced Search

Journal of Structural Chemistry

2009 year, number 5

STRUCTURE OF Ir-Al2O3 COATINGs OBTAINED BY CHEMICAL VAPOR DEPOSITION IN THE HYDROGEN ATMOSPHERE

N. V. Gelfond, N. B. Morozova, I. K. Igumenov, E. S. Filatov, S. A. Gromilov, R. I. Kvon
Keywords: Ir and Ir-Al2O3 composite coatings, chemical vapor deposition, iridium(III), aluminum(III), tris-acetylacetonates
Pages: 955-959

Abstract

Chemical vapor deposition is used to obtain Ir and Ir-Al2O3 coatings with a thickness of up to 5 μm and growth rate of 2.5 μm/h on steel substrates previously covered with an alumina layer. Tris-acetylacetonates of Ir(III) and Al(III) are used as precursors. The deposition process is carried out at the atmospheric pressure in the presence of hydrogen. The coatings obtained are studied by X-ray diffraction, X-ray photoelectron spectroscopy, and scanning electron microscopy. A dependence of the structure and composition of coatings on their preparation conditions is found.