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Journal of Structural Chemistry

2009 year, number 2

NEW POLYMORPHIC MODIFICATION OF THE CRYSTAL STRUCTURE OF BROMOPEGANOL

R. Y. Okmanov, A. G. Tozhiboev, K. K. Turgunov, B. Tashkhodzhaev, N. I. Mukarramov, K. M. Shakhidoyatov
Keywords: alkaloids, quinazolines, polymorphism, X-ray diffraction analysis
Pages: 396-398

Abstract

The crystal structure of 6-bromopeganol in a new polymorphic modification is found and determined by single crystal X-ray diffraction analysis. For the crystal structure of the new polymorph the formation of a centrosymmetric closed dimer (associate) is also characteristic. It consists of two bromopeganol molecules bound by centrosymmetric reciprocal hydrogen bonds O-H…N(1). This polymorph differs from the known one in the mutual arrangement and interaction of these associates.