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Chemistry for Sustainable Development

2005 year, number 2

Obtaining the Composite MoB Material by Means of Force SHS Compacting with Preliminary Mechanical Activation of Mo-10 % B Mixture

E. N. EREMINA, V. V. KURBATKINA, E. A. LEVASHOV, A. S. ROGACHEV and N. A. KOCHETOV
Moscow State Institute of Steel and Alloys, Leninskiy pr. 4, Moscow 119049 (Russia)
Institute of Structural Macrokinetics and Materials Science, SHS Scietific Training Centre,
Chernogolovka 142432, Moscow Region (Russia) E-mail: vvkurb@mail.ru
Pages: 197-204

Abstract

The reactivity of the mixture Mo-10 % B is investigated, along with the effect of the parameters of mechanical activation on heat evolution, specific surface, structure of powders, activation energy of combustion process, heat evolution rate, temperature and rate of combustion. It is shown that activation in the optimal regimes increases the reactivity of low-exothermal mixture Mo-10 % B. Using the technology of force compaction, a multilayer composite target for magnetron sputtering was obtained. It was established that the density and hardness of the synthesized material increase in the case if preliminary mechanical activation is applied.