CRYSTAL STRUCTURE OF (2-CHLORO-4-(PHENYLTHIO)PHENYL)(3-METHYL-1-PHENYL-5-(PHENYLTHIO)-1H-PYRAZOL-4-YL)METHANONE
G.-X. Sun1, Z.-W. Zhai2, Z.-H. Sun2, C.-X. Tan2, J.-Q. Weng2, X.-H. Liu2
1chool of Chemistry and Chemical Engineering, Yancheng Institute of Technology, Jiangsu, Yancheng, P. R. China
2College of Chemical Engineering, Zhejiang University of Technology, Hangzhou, Zhejiang, P. R. China
xhliu@zjut.edu.cn
Ключевые слова: aryl sulfide, synthesis, crystal structure
Страницы: 1713-1717
Аннотация
(2-Chloro-4-(phenylthio)phenyl)(3-methyl-1-phenyl-5-(phenylthio)-1H-pyrazol-4-yl)methanone was obtained by accident. In order to know the structure of this product, the compound was isolated by column chromatography and recrystallized from EtOH. The compound was characterized by X-ray diffraction. The compound crystallized in the triclinic space group P -1 with a = 9.909(2), b = 11.824(2), c = 13.056(3) Å, a = 63.309(3)°, b = 89.964(4)°, g = 67.727(3)°, V = 1237.7(4) Å3, Z = 2 and R = 0.0414.
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