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Journal of Structural Chemistry

2014 year, number 2

TWO CRYSTAL MODIFICATIONS OF [PdEn(NO2)2]. SYNTHESIS, STRUCTURE, AND THERMAL PROPERTIES

S. P. Khranenko1, N. V. Kuratieva1,2, P. E. Plyusnin1,2, S. A. Gromilov1,2
1Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia
2Novosibirsk State University, Novosibirsk, Russia
Keywords: palladium, ethylenediamine, complex compounds, single crystal X-ray diffraction study, crystal chemistry, thermal properties

Abstract

The crystal structure of two modifications of [PdEn(NO2)2] is determined by single crystal X-ray diffraction. The geometric characteristics of the complexes and the motifs of their mutual arrangement in the structures are compared. The thermal properties in different gaseous atmospheres are studied.