CRYSTAL STRUCTURE OF ETHYL 9-METHYL-10- PHENYL-11-THIOXO-8-OXA-10,12-DIAZATRICYCLO[7.3.1.02.7] TRIDECA-2(7),3,5-TRIEN-13-CARBOXYLATE
A. M. Magerramov, A. V. Kurbanov, V. N. Khrustalev, S. S. Godzhaeva, Г‰. N. Garibov, V. M. Farzaliev, M. A. Allakhverdiev
Keywords: single crystal X-ray diffraction, crystal structure, ethyl 9-methyl-10-phenyl-11-thioxo-8-oxa-10, 12-diazatricyclo[7.3.1.02.7]trideca-2(7), 3, 5-trien-13-carboxylate, N1-phenylthiocarbamide
Pages: 999-1002
Abstract
Three-component condensation of N1-phenylthiocarbamide with salicylaldehyde and with the ether of acetoacetic acid in the presence of trifluoroacetic acid provides a productive synthesis of ethyl 9-methyl-10-phenyl-11-thioxo-8-oxa-10,12-diazatricyclo[7.3.1.02.7]trideca-2(7),3,5-trien-13-carboxylate I. Single crystal XRD is used to determine the crystal structure of I and to identify the conformation properties of the structures.
|
